HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → Ethyl 2-(4-bromo-2-oxopyridin-1(2H)-YL)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | 4-Bromo-2-hydroxypyridine | HCID 817115 | — |
| Product | Ethyl 2-(4-bromo-2-oxopyridin-1(2H)-YL)acetate | HCID 71009808 | — |
Reaction Steps
5.0 g (28.7 mmol) of 4-bromopyridin-2(1H)-one and 5.3 g (31.6 mmol) of ethyl bromoacetate were reacted according to General Method 4B. Yield: 6.2 g (83% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434690B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-3afa27d21b1c4117801cdffa704044f9 |
| Source note | uspto-grants-2016_09 |