HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 21263751, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 21263747 | HCID 21263747 | — |
| Product | HCID 21263751 | HCID 21263751 | 86% |
Reaction Steps
A mixture of 4,6,6-trimethyl-1-cyclohexene-1-methanol (3 g, 19.5 mmole) and acetic anhydride (2.4 g, 24 mmole) was heated to 70° during 3 h, then distilled at a bath temperature of 70°/0.5 hPa, to obtain 3.27 g (86%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06177400B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-380ad4c6b05642ed9126da1473f201a3 |
| Source note | uspto-grants-2001_01 |