HCID 18616992, compound → HCID 135673410, compound

Participants

Reaction Steps

6-(2-Hydroxy-5-methoxyphenyl)-6′-(2-hydroxy-3-methoxy-5-methylphenyl)-2,2′-bipyridine was prepared from 6-bromo-6′-(2-hydroxy-5-methoxyphenyl)-2,2′-bipyridine and 2-hydroxy-3-methoxy-5-methylphenylboronic acid in 43% yield using method F; δH [2H6]-DMSO 13.40,(1H, s), 12.51,(1H, s), 8.37,(1H, d), 8.29,(1H, d), 8.20,(2H, t), 8.14,(2H, d), 7.67,(1H, s), 7.51,(1H, s), 7.00,(1H, d), 6.94,(2H, m), 3.83,(6H, s), 2.34,(3H, s).

Provenance & Evidence