HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H,3H-Naphtho(1,8-cd)pyran-1,3-dione, 6-bromo- → HCID 22624038, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H,3H-Naphtho(1,8-cd)pyran-1,3-dione, 6-bromo- | HCID 66493 | — |
| Reactant | Benzyloxyamine hydrochloride | HCID 102312 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 22624038 | HCID 22624038 | 87.2% |
Reaction Steps
O-Benzyl hydroxylamine hydrochloride (2.0 g, 12.5 mmol) and 4-bromo-1,8-naphthalic anhydride (2.9 g, 10.5 mmol) were reacted in pyridine (50 mL) following the procedure of Example D to give 3.5 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06177423B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-3aef29a4c6f249d3aa331bf3e433efb1 |
| Source note | uspto-grants-2001_01 |