HRID567070

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：COCCN(C1CC(C)(C)Oc2ccc(OCc3ccccc3)cc21)S(C)(=O)=O

HCID21264516

未命名化合物

PRODUCTS

生成物

结构：COCCN(C1CC(C)(C)Oc2ccc(O)cc21)S(C)(=O)=O

HCID17786848

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID178418390

未命名化合物

溶剂HCID21899815

未命名化合物

PROCEDURE

实验过程

6 g of N-[6-benzyloxy-2,2-dimethylchroman-4-yl]-N-(2-methoxyethyl)methanesulfonamide were dissolved in 100 ml of THF/methanol (1:1) and hydrogenated in a shaking duck using Pd/carbon. The crude product was crystallized using diisopropyl ether, 4.6 g, m.p. 115-117° C.

WORKUP

后处理

customThe crude product was crystallized