HCID 59941051, compound → HCID 9868784, compound

HRID 567071Notes

Reaction equation

HRID 567071 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][N:5]([S:27]([CH3:30])(=[O:29])=[O:28])[CH:6]1[C:15]2[C:10](=[CH:11][CH:12]=[C:13]([O:16][CH2:17][CH2:18][CH2:19][C:20](OCC)=[O:21])[CH:14]=2)[O:9][C:8]([CH3:26])([CH3:25])[CH2:7]1>NCCO>[OH:2][CH2:3][CH2:4][NH:5][C:20](=[O:21])[CH2:19][CH2:18][CH2:17][O:16][C:13]1[CH:14]=[C:15]2[C:10](=[CH:11][CH:12]=1)[O:9][C:8]([CH3:26])([CH3:25])[CH2:7][CH:6]2[N:5]([S:27]([CH3:30])(=[O:28])=[O:29])[CH2:4][CH2:3][O:2][CH3:1]

Participants

3

Reactant 1

HCID 59941051HCID 59941051, compound

Product 1

HCID 9868784HCID 9868784, compound

Reagents, catalysts & solvents 1

HCID 700EthanolamineSolvent

Procedure

0.55 g of ethyl 4-[4-((2-methoxyethyl)methanesulfonylamino)-2,2-dimethylchroman-6-yloxy]butyrate (Example 19a) was reacted at 90° C. for 2 h in 4 ml of 2-aminoethanol, 0.6 g of oily product.

Sources & evidence

ORD record
ord-9447f6dabc474327be3e26be377e50ac
Source dataset
uspto-grants-2001_01
Patent number
US06177449B1

Reaction notes

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