HCID 21264512, compound → HCID 17786842, compound

HRID 567074Notes

Reaction equation

HRID 567074 reaction equation
C([O:8][C:9]1[CH:10]=[C:11]2[C:16](=[CH:17][CH:18]=1)[O:15][C:14]([CH3:20])([CH3:19])[CH2:13][CH:12]2[N:21]([CH2:27][CH2:28][CH3:29])[S:22]([CH2:25][CH3:26])(=[O:24])=[O:23])C1C=CC=CC=1>C1COCC1.CO>[CH3:20][C:14]1([CH3:19])[CH2:13][CH:12]([N:21]([CH2:27][CH2:28][CH3:29])[S:22]([CH2:25][CH3:26])(=[O:24])=[O:23])[C:11]2[C:16](=[CH:17][CH:18]=[C:9]([OH:8])[CH:10]=2)[O:15]1

Participants

3

Reactant 1

HCID 21264512HCID 21264512, compound

Product 1

HCID 17786842HCID 17786842, compound

Reagents, catalysts & solvents 1

HCID 21899815MeOH tetrahydrofuranSolvent

Procedure

6.0 g of N-[6-benzyloxy-2,2-dimethylchroman-4-yl]-N-(1-propyl)ethanesulfonamide were dissolved in 150 ml of THF/methanol (1:1) and hydrogenated in a shaking duck using Pdlcarbon, 4.4 g of product, m.p. 173-175° C. (from petroleum ether).

Sources & evidence

ORD record
ord-5e672178a0f642089ca8cc35f337e84b
Source dataset
uspto-grants-2001_01
Patent number
US06177449B1

Reaction notes

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