HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Anisoyl chloride → HCID 9866654, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 2739390 | HCID 2739390 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 9866654 | HCID 9866654 | 101.3% |
Reaction Steps
4-(4-Trifluoromethylphenyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridine (100 mg, 0.35 mmol) was dissolved in dichloromethane (0.5 mL) and triethylamine (0.5 mL) was added. To this solution p-anisoyl chloride (60 mg, 0.35 mmol) dissolved in dichloromethane (0.5 ml) was added in one portion. The mixture was filtered and evaporated to afford 148 mg (100%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06177443B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-76a3b8b966894c90b9ef97dac0b7ecc9 |
| Source note | uspto-grants-2001_01 |