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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 567092Generated: October 31, 2026

p-Anisoyl chloride → HCID 9866654, compound

https://huagongshe.com/reaction/567092

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp-Anisoyl chlorideHCID 7477—
ReactantTriethylamineHCID 8471—
ReactantHCID 2739390HCID 2739390—
SolventDichloromethaneHCID 6344—
ProductHCID 9866654HCID 9866654101.3%

Reaction Steps

4-(4-Trifluoromethylphenyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridine (100 mg, 0.35 mmol) was dissolved in dichloromethane (0.5 mL) and triethylamine (0.5 mL) was added. To this solution p-anisoyl chloride (60 mg, 0.35 mmol) dissolved in dichloromethane (0.5 ml) was added in one portion. The mixture was filtered and evaporated to afford 148 mg (100%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06177443B1
Source datasetuspto-grants-2001_01
ORD IDord-76a3b8b966894c90b9ef97dac0b7ecc9
Source noteuspto-grants-2001_01