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HRID56711

反应详情

EQUATION

反应方程式

HRID 56711 的结构方程式

REACTANTS

反应物

2
结构：CC(Br)C(=O)OC(C)(C)C
HCID545327

tert-Butyl 2-bromopropanoate

C7H13BrO2

结构：O=c1cc(-c2cc(Cl)ccc2C(F)(F)F)c(Cl)c[nH]1
HCID117605078

未命名化合物

PRODUCTS

生成物

1
结构：CC(C(=O)OC(C)(C)C)n1cc(Cl)c(-c2cc(Cl)ccc2C(F)(F)F)cc1=O
HCID117622552

未命名化合物

PROCEDURE

实验过程

123 mg (0.4 mmol) of 5-chloro-4-[5-chloro-2-(trifluoromethyl)phenyl]pyridin-2(1H)-one and 1.05 eq. of tert-butyl 2-bromopropanoate (racemate) were reacted according to General Method 4B at 100° C. Yield: 81 mg (47% of theory)

WORKUP

后处理

  1. customaccording to General Method 4B at 100° C