反应详情

A solution of 3-(4-methoxyphenyl)propan-1-ol (15.02 g) in dichloromethane (100 ml) was added to a stirred suspension of pyridinium chlorochromate (29 g) in dichloromethane (250 ml). The mixture was stirred for 2 hours then filtered through a kieselguhr pad. The residue was washed with ether (3×500 ml) and the combined liquors were evaporated under reduced pressure. The residual oil was purified by vacuum distillation to give the subtitle compound (6.81 g) as an oil.

1. filtrationthen filtered through a kieselguhr pad
2. washThe residue was washed with ether (3×500 ml)
3. customthe combined liquors were evaporated under reduced pressure
4. distillationThe residual oil was purified by vacuum distillation