HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromophenyl isocyanate → N-(2-hydroxy-4-nitrophenyl)-N'-(4-bromophenyl)urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromophenyl isocyanate | HCID 75609 | — |
| Reactant | 2-Amino-5-Nitrophenol | HCID 4984721 | — |
| Product | N-(2-hydroxy-4-nitrophenyl)-N'-(4-bromophenyl)urea | HCID 21184636 | 37% |
Reaction Steps
N-(2-Hydroxy-4-nitrophenyl)-N′-(4-bromophenyl)urea was prepared from 2-hydroxy 4-nitro aniline (500 mg, 3.24 mmol) and 4-bromophenylisocyanate (3.24 mmol) according to the procedure in General Method B. The product was purified by dilution with methylene chloride and precipitation with hexanes. Filtering afforded the title compound(0.41 g, 37%). EI-MS m/z 352(M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06180675B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-52f245df686142b596506ebeb4e98972 |
| Source note | uspto-grants-2001_01 |