HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromophenyl isocyanate → HCID 53798129, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromophenyl isocyanate | HCID 137097 | — |
| Reactant | Benzoic acid, 4-amino-3-hydroxy-, methyl ester | HCID 7020619 | — |
| Product | HCID 53798129 | HCID 53798129 | 33% |
Reaction Steps
The urea was prepared from 2-hydroxy 4-carbomethoxy aniline(0.167 g, 1 mmol) and 2-bromophenylisocyanate(1 mmol) by general Method B. It was purified by dilution with methylene chloride and precipitation with hexane. Filtering afforded the desired compound(0.12 g, 33%). EI-MS m/z 363(M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06180675B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-1cb32509e6664f738366d67ca0cf5a98 |
| Source note | uspto-grants-2001_01 |