HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromophenyl isocyanate → HCID 22011338, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromophenyl isocyanate | HCID 137097 | — |
| Reactant | 2-Amino-5-fluorophenol | HCID 185763 | — |
| Product | HCID 22011338 | HCID 22011338 | — |
Reaction Steps
The urea was prepared from 2-hydroxy 4-fluoro aniline(254 mg, 2 mmol) and 2-bromophenylisocyanate by general Method B. It was purified by dilution with methylene chloride and precipitation with hexane(173 mg, 26%). EI-MS m/z 325 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06180675B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-33079978df534ffa833de2b9f7054160 |
| Source note | uspto-grants-2001_01 |