HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1,1'-Biphenyl)-3-ol, 4-nitro- → 2-Amino-5-phenylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1,1'-Biphenyl)-3-ol, 4-nitro- | HCID 87437 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Amino-5-phenylphenol | HCID 20376 | — |
Reaction Steps
A solution of 2-nitro 5-phenylphenol(1.2 g, 5.5 mmol) in methanol was treated with 10% Pd/C(1.2 g). The reaction mixture was flushed with hydrogen and allowed to stir overnight. The reaction mixture was filtered through celite and the filtrate was concentrated in vacuo to afford desired (1.01 g, 98%). EI-MS m/z 186(M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06180675B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-ae3410ffb02b4a9a92724183a1fd4f28 |
| Source note | uspto-grants-2001_01 |