HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-methylphenol → HCID 22011341, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-methylphenol | HCID 76082 | — |
| Reactant | 2-Bromophenyl isocyanate | HCID 137097 | — |
| Product | HCID 22011341 | HCID 22011341 | — |
Reaction Steps
The urea was prepared from 2-hydroxy 4-methyl aniline(0.274 g, 2 mmol) and 2-bromo phenylisocyanate(0.40 g, 2 mmol) by general Method B. It was purified by dilution of the DMF solution with methylene chloride and precipitation with hexane(249 mg, 39%). EI-MS m/z 319(M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06180675B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-440de0972e0a4afe842cb82fe9ba3594 |
| Source note | uspto-grants-2001_01 |