HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → HCID 54436784, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | N-Acetylsulfanilyl chloride | HCID 8481 | — |
| Product | HCID 54436784 | HCID 54436784 | — |
Reaction Steps
The sulfonamide was synthesized from 4-acetamidophenyl sulfonyl chloride(0.01 mol) and o-phenylene diamine(0.01 mol) by general Method C. It was purified by recrystallization from EtOH(1.27 g,40%)EI-MS m/z 304(M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06180675B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-b112d113f5b84be6ae5e1fa3928efc1b |
| Source note | uspto-grants-2001_01 |