HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → N-(2-Aminophenyl)-3-methylbenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | 3-Methylbenzenesulphonyl chloride | HCID 2734595 | — |
| Product | N-(2-Aminophenyl)-3-methylbenzenesulfonamide | HCID 16773320 | — |
Reaction Steps
The sulfonamide was synthesized from 3-tolylsulfonyl chloride(0.01 mol) and o-phenylene diamine(0.01 mol) by general Method C. It was purified by recrystallization from EtOH(0.73g, 28%). EI-MS m/z 263 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06180675B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-fb97612670f04d55ad3bc8c875985fe4 |
| Source note | uspto-grants-2001_01 |