HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromophenyl isocyanate → HCID 53843945, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromophenyl isocyanate | HCID 137097 | — |
| Reactant | HCID 21263225 | HCID 21263225 | — |
| Product | HCID 53843945 | HCID 53843945 | 46.2% |
Reaction Steps
The urea was synthesized from 2-((8-quinolinyl)sulfonylamino)aniline(1 mmol) and 2-bromophenylisocyanate(1 mmol) by general Method B. It was purified by dilution with methylene chloride and precipitation with hexane. Filtering afforded the desired compound(0.23 g, 46%). EI-MS m/z 495(M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06180675B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-ffb53ea5bd2d4c0b8970be169f74e8a0 |
| Source note | uspto-grants-2001_01 |