HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178478837, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,4-Diphenyl-1,4-butanedione | HCID 136322 | — |
| Reactant | HCID 178513185 | HCID 178513185 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178478837 | HCID 178478837 | — |
Reaction Steps
1,2-dibenzoylethane (4.76 g), aminoguanidine bicarbonate (5.45 g), and concentrated hydrochloric acid (3.33 mL) were heated in 50% ethanol (60 mL) for 24 hr. Cooling, concentration and filtration gave 4.3 g of 2,2′-(1,4-diphenyl-1,4-butanediylidene)bis(hydrazinecarboximidamide) dihydrochloride, mp 285-6° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06180676B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-89ced001b3d7404f849e7d3ea810af34 |
| Source note | uspto-grants-2001_01 |