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HRID568260

反应详情

EQUATION

反应方程式

HRID 568260 的结构方程式

REACTANTS

反应物

3
结构：C=CCOC(=O)N1C[C@@H](SC(C)=O)C[C@H]1C(=O)O
HCID15299255

未命名化合物

结构：CNCc1ncc2sccn12
HCID21262403

未命名化合物

结构：C[N+](C)=CCl.ClCCl.[Cl-]
HCID131722372

未命名化合物

PRODUCTS

生成物

1
结构：C=CCOC(=O)N1C[C@@H](SC(C)=O)C[C@H]1C(=O)N(C)Cc1ncc2sccn12
HCID20639589

未命名化合物

收率 47.4%

PROCEDURE

实验过程

The procedure of Synthesis Example 1 is repeated, except that 260 mg of (3S,5S)-3-acetylthio-1-allyloxycarbonylpyrrolidin-5-carboxylic acid, 0.95 ml of a 1.1 M Vilsmeier reagent/dichloromethane solution, and 159 mg of 5-(N-methylaminomethyl)imidazo[5,1-b]thiazole. Thus, 190.6 mg of the title compound is prepared as a slightly yellow amorphous material.

WORKUP

后处理

  1. customThe procedure of Synthesis Example 1