Thionyl Chloride → 4-(Chlorocarbonyl)phenyl nonanoate

HRID 568319Notes

Reaction equation

HRID 568319 reaction equation
[CH2:1]([C:9]([O:11][C:12]1[CH:20]=[CH:19][C:15]([C:16](O)=[O:17])=[CH:14][CH:13]=1)=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S(Cl)([Cl:23])=O>C(Cl)(Cl)(Cl)Cl>[CH2:1]([C:9]([O:11][C:12]1[CH:20]=[CH:19][C:15]([C:16]([Cl:23])=[O:17])=[CH:14][CH:13]=1)=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 35638214-(Nonanoyloxy)benzoic acid

Product 1

HCID 135310434-(Chlorocarbonyl)phenyl nonanoate

Reagents, catalysts & solvents 1

HCID 5943Carbon TetrachlorideSolvent

Procedure

2.5 g of 4-octylcarbonyloxybenzoic acid was dispersed in 50 ml carbon tetrachloride, after dropping 10 ml of thionyl chloride to this solution, refluxed for three hours. After reducing the solvent, 4-octylcarbonyloxybenzoic chloride (CK) was obtained.

Workup

  1. temperaturerefluxed for three hours

Sources & evidence

ORD record
ord-1f806c24745a4aa7998fab230fe446ec
Source dataset
uspto-grants-1988_03
Patent number
US04728458

Reaction notes

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