huagongshe.com
HRID568319

反应详情

EQUATION

反应方程式

HRID 568319 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：CCCCCCCCC(=O)Oc1ccc(C(=O)O)cc1
HCID3563821

Benzoic acid, 4-[(1-oxononyl)oxy]-

C16H22O4

PRODUCTS

生成物

1
结构：CCCCCCCCC(=O)Oc1ccc(C(=O)Cl)cc1
HCID13531043

4-(Chlorocarbonyl)phenyl nonanoate

C16H21ClO3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)(Cl)Cl
溶剂HCID5943

Carbon tetrachloride

CCl4

PROCEDURE

实验过程

2.5 g of 4-octylcarbonyloxybenzoic acid was dispersed in 50 ml carbon tetrachloride, after dropping 10 ml of thionyl chloride to this solution, refluxed for three hours. After reducing the solvent, 4-octylcarbonyloxybenzoic chloride (CK) was obtained.

WORKUP

后处理

  1. temperaturerefluxed for three hours