4-(4-Nitro-3-trifluoromethylphenyl)-1,2,4-triazole → 4-(4-Amino-3-trifluoromethylphenyl)-1,2,4-triazole

HRID 568388Notes

Reaction equation

HRID 568388 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([N:10]2[CH:14]=[N:13][N:12]=[CH:11]2)=[CH:6][C:5]=1[C:15]([F:18])([F:17])[F:16])([O-])=O.C.[H][H]>>[NH2:1][C:4]1[CH:9]=[CH:8][C:7]([N:10]2[CH:11]=[N:12][N:13]=[CH:14]2)=[CH:6][C:5]=1[C:15]([F:18])([F:17])[F:16]

Participants

3

Reactant 2

HCID 198670904-(4-Nitro-3-trifluoromethylphenyl)-1,2,4-triazoleHCID 178477803HCID 178477803, compound

Product 1

HCID 198670854-(4-Amino-3-trifluoromethylphenyl)-1,2,4-triazole

Procedure

The following compound, m.p. 196°-8°, was prepared similarly to the previous Preparation using 4-(4-nitro-3-trifluoromethylphenyl)-1,2,4-triazole and 5% palladised charcoal/H2 as the starting materials: ##STR137##

Workup

  1. customThe following compound, m.p. 196°-8°, was prepared similarly to the previous Preparation

Sources & evidence

ORD record
ord-5284a0c1de654a6e9cfde75908dd5d52
Source dataset
uspto-grants-1988_03
Patent number
US04728653

Reaction notes

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