HRID568389

反应详情

EQUATION

反应方程式

HRID 568389 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The following compound was prepared similarly to Preparation 56, using 1-(3-methyl-4-nitrophenyl)-2,4-dimethylimidazole and 5% palladised charcoal/H2 as the starting materials and ethanol as the solvent. The crude solid melted at 78°-82°. Recrystallisation from toluene gave 1-(4-amino-3-methylphenyl)-2,4-dimethylimidazole, m.p. 118°-120° C.

WORKUP

后处理

  1. customThe following compound was prepared similarly to Preparation 56
  2. customRecrystallisation from toluene