1-Piperazinecarboxaldehyde → HCID 178521669, compound

HRID 568457Notes

Reaction equation

HRID 568457 reaction equation
Cl[C:2]1[N:3]=[C:4]([N:13]2[CH2:18][CH2:17][O:16][CH2:15][CH2:14]2)[C:5]2[N:11]=[CH:10][N:9]=[C:8]([SH:12])[C:6]=2[N:7]=1.[CH:19]([N:21]1[CH2:26][CH2:25][NH:24][CH2:23][CH2:22]1)=[O:20]>>[CH:19]([N:21]1[CH2:26][CH2:25][N:24]([C:2]2[N:3]=[C:4]([N:13]3[CH2:18][CH2:17][O:16][CH2:15][CH2:14]3)[C:5]3[N:11]=[CH:10][N:9]=[C:8]([SH:12])[C:6]=3[N:7]=2)[CH2:23][CH2:22]1)=[O:20]

Participants

3

Reactant 2

HCID 821911-PiperazinecarboxaldehydeHCID 178527886HCID 178527886, compound

Product 1

HCID 178521669HCID 178521669, compound

Procedure

This compound was prepared analogous to Example 93 from 2-chloro-8-mercapto-4-morpholino-pyrimido-[5,4-d]-pyrimidine (m.p.: >300° C., decomp.) and N-formyl-piperazine.

Sources & evidence

ORD record
ord-4942043141564a10b7c834fdc0d739d4
Source dataset
uspto-grants-1988_03
Patent number
US04728646

Reaction notes

Loading…