HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178478516, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1H-Imidazole-1-octanamine | HCID 13952861 | — |
| Reactant | 2-Methylthiobenz(cd)indole hydriodide | HCID 20150650 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178478516 | HCID 178478516 | — |
Reaction Steps
A mixture of 2.1 g of 8-(1H-imidazol-1-yl)octanamine, 400 ml of ethanol, and 3.2 g of 2-(methylthio)benz[cd]indole hydroiodide was reacted as described in Example 19, giving the base derivative which was then treated with hydrochloric acid giving 1.3 g of the desired hydrochloride salt, mp 222°-224° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04728663 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-abe069862a2e420a97df30ebbc44e8ff |
| Source note | uspto-grants-1988_03 |