HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(1H-Imidazol-1-yl)butan-1-amine → 6-bromo-N-(3-imidazol-1-ylbutyl)benzo[cd]indol-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(1H-Imidazol-1-yl)butan-1-amine | HCID 13952862 | — |
| Reactant | HCID 178527759 | HCID 178527759 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 6-bromo-N-(3-imidazol-1-ylbutyl)benzo[cd]indol-2-amine | HCID 178448831 | 41.3% |
Reaction Steps
A mixture of 5.2 g of 6-bromo-benz[cd]indole-2-thiol, 2.8 g of 3-(1H-imidazol-1-yl)butanamine, 6.6 g of mercuric acetate and 100 ml of dry p-dioxane was reacted as described in Example 1, giving 3.0 g of the desired product, mp 240°-241° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04728663 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-bb3dad1699d04907803579142e48da58 |
| Source note | uspto-grants-1988_03 |