HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Imidazole-1-propanamine → 2-(3-imidazol-1-ylpropylamino)-N,N-dimethylbenzo[cd]indole-6-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Imidazole-1-propanamine | HCID 78736 | — |
| Reactant | 1,2-dihydro-N,N-dimethyl-2-thioxobenz(cd)indole-6-sulfonamide | HCID 19914607 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(3-imidazol-1-ylpropylamino)-N,N-dimethylbenzo[cd]indole-6-sulfonamide | HCID 178486128 | 41.2% |
Reaction Steps
A mixture 5 g of 1,2-dihydro-N,N-dimethyl-2-thioxobenz[cd]indole-6-sulfonamide, 2.3 g of 3-(1H-imidazol-1-yl)propanamine, 100 ml of ethanol and 5.4 g of mercuric acetate was reacted as described in Example 1, giving 2.7 g of the desired product, mp 199°-201° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04728663 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-a6d88a60759844b4b026e6e315e6273a |
| Source note | uspto-grants-1988_03 |