Ethanol → HCID 178448846, compound

HRID 568498Notes

Reaction equation

HRID 568498 reaction equation
[Cl:1][C:2]1[C:3]2[C:4]3[C:8](=[C:9]([Cl:11])[CH:10]=1)[N:7]=[C:6](S)[C:5]=3[CH:13]=[CH:14][CH:15]=2.[N:16]1([CH2:21][CH2:22][CH:23]([NH2:25])C)[CH:20]=[CH:19][N:18]=[CH:17]1.[CH2:26](O)C>>[Cl:1][C:2]1[C:3]2[C:4]3[C:8](=[C:9]([Cl:11])[CH:10]=1)[N:7]=[C:6]([NH:25][CH2:23][CH2:22][CH:21]([N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1)[CH3:26])[C:5]=3[CH:13]=[CH:14][CH:15]=2

Participants

4

Reactant 3

HCID 702EthanolHCID 136181154-(1H-imidazol-1-yl)-2-butanamineHCID 178527805HCID 178527805, compound

Product 1

HCID 178448846HCID 178448846, compound

Procedure

A mixture of 7.0 g of 6,8-dichloro-benz[cd]indole-2-thiol, 100 ml of ethanol, 9.5 g of mercuric acetate and 4.2 g of 4-(1H-imidazol-1-yl)-2-butanamine was reacted as described in Example 1, giving 1.7 g of the desired product, mp 244°-246° C. (dec.).

Workup

  1. customwas reacted

Sources & evidence

ORD record
ord-305596e08e4540f9b5fc4200dd6bbc7b
Source dataset
uspto-grants-1988_03
Patent number
US04728663

Reaction notes

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