HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Imidazole-1-propanamine → 6,8-dichloro-N-(3-imidazol-1-ylpropyl)benzo[cd]indol-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Imidazole-1-propanamine | HCID 78736 | — |
| Reactant | HCID 178527805 | HCID 178527805 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 6,8-dichloro-N-(3-imidazol-1-ylpropyl)benzo[cd]indol-2-amine | HCID 178478174 | 43.4% |
Reaction Steps
A mixture of 5.0 g of 6,8-dichloro-benz[cd]indole-2-thiol, 35 ml of dimethylformamide, 2.6 g of 3-(1H-imidazol-yl)propanamine and 6.3 g of mercuric acetate was reacted as described in Example 1, giving 2.95 g of the desired product, mp 182°-183° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04728663 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-894f03992644433380b4a35ecbc244c8 |
| Source note | uspto-grants-1988_03 |