HRID568582

反应详情

EQUATION

反应方程式

HRID 568582 的结构方程式

PROCEDURE

实验过程

204 g of allylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride (isomeric mixture) are reacted with 103 g of neopentanolamine at 120° C. for 4 hours, and the product is distilled. There is obtained between 169° and 172° C. at 2.53 Pa 268 g (92.7% of theory) of a yellow oil having a refractive index n25D of 1.5190 and a viscosity of 6.21 Pa.s.

WORKUP

后处理

  1. distillationthe product is distilled
  2. customThere is obtained between 169° and 172° C. at 2.53 Pa 268 g (92.7% of theory) of a yellow oil