1-Propanol, 3-amino-2,2-dimethyl- → HCID 178438303, compound

HRID 568582Notes

Reaction equation

HRID 568582 reaction equation
[CH2:1]([C:4]12[CH2:10][CH:7]([CH:8]=[CH:9]1)[CH:6]1[C:11]([O:13][C:14](=[O:15])[CH:5]21)=[O:12])[CH:2]=[CH2:3].[CH3:16][C:17]([CH2:21][OH:22])([CH2:19][NH2:20])[CH3:18]>>[CH3:16][C:17]([CH3:18])([CH2:21][OH:22])[CH2:19][N:20]=[C:14]([CH:5]1[CH:6]([C:11]([OH:13])=[O:12])[CH:7]2[CH2:10][C:4]1([CH2:1][CH:2]=[CH2:3])[CH:9]=[CH:8]2)[OH:15]

Participants

3

Reactant 2

HCID 1173261-Propanol, 3-amino-2,2-dimethyl-HCID 54206110Allylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride

Product 1

HCID 178438303HCID 178438303, compound

Procedure

204 g of allylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride (isomeric mixture) are reacted with 103 g of neopentanolamine at 120° C. for 4 hours, and the product is distilled. There is obtained between 169° and 172° C. at 2.53 Pa 268 g (92.7% of theory) of a yellow oil having a refractive index n25D of 1.5190 and a viscosity of 6.21 Pa.s.

Workup

  1. distillationthe product is distilled
  2. customThere is obtained between 169° and 172° C. at 2.53 Pa 268 g (92.7% of theory) of a yellow oil

Sources & evidence

ORD record
ord-a1f1c82c01ab46c7a763f2129e614b10
Source dataset
uspto-grants-1988_03
Patent number
US04728742

Reaction notes

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