Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diglycolamine | HCID 13578 | — |
| Reactant | Allylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride | HCID 54206110 | — |
| Product | HCID 178438305 | HCID 178438305 | — |
Reaction Steps
120 g of allylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride (isomeric mixture) are reacted at 140° C. with 67.9 g of diglycolamine; the mixture is heated to 200° C. and the pressure lowerd to 10.6 Pa. The yield is 142.6 g of a yellow oil having a viscosity of 1.55 Pa.s at 25° C. and an n25D of 1.5230.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04728742 |
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| Source dataset | uspto-grants-1988_03 |
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| ORD ID | ord-1eb56e47d2334be785f53fec6461a47d |
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| Source note | uspto-grants-1988_03 |
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