HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dichloroanisole → HCID 14012560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dichloroanisole | HCID 16126 | — |
| Reactant | 2-Chlorobenzoyl chloride | HCID 69110 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | HCID 14012560 | HCID 14012560 | — |
Reaction Steps
The Friedel-Crafts procedure of Example 24a is repeated with 48.13 g of o-chlorobenzoyl chloride being combined with 36.7 g AlCl3 and 44.26 g of 2,3-dichloroanisole to yield a white crystalline product of 2,3-dichloro-4-methoxy-2'-chlorobenzophenone, mp 117°-120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04728662 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-9f64bfd932b14a1fbf039f0756fd57b2 |
| Source note | uspto-grants-1988_03 |