HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Benzyloxybenzoylchloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-(Benzyloxy)benzoic acid | HCID 73880 | — |
| Product | 4-Benzyloxybenzoylchloride | HCID 3766410 | 58.4% |
Reaction Steps
Thionyl chloride (63.1 g, 0.53 mol) was added to p-benzyloxybenzoic acid (100.0 g, 0.44 mol), followed by refluxing the mixture for about 2 hours, and completely removing excess thionyl chloride by distillation under reduced pressure to obtain p-benzyloxybenzoic acid chloride (63.4 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04729847 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-a4e0a30e8bcd43c481dbffadee5ac192 |
| Source note | uspto-grants-1988_03 |