HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 13878422, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | p-(1-Methyl-heptyloxy)benzoic acid | HCID 13878419 | — |
| Product | HCID 13878422 | HCID 13878422 | 93% |
Reaction Steps
Thionyl chloride (51.2 g, 0.43 mol) was added to optically active p-(1-methyl-heptyloxy)benzoic acid (90.0 g, 0.36 mol), followed by refluxing the mixture for about 2 hours, thereafter completely removing excess thionyl chloride by distillation under reduced pressure to obtain optically active p-(1-methyl-heptyloxy)benzoic acid chloride (90.0 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04729847 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-a514f906415d486db0b095e432061e79 |
| Source note | uspto-grants-1988_03 |