HRID568758

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID68516

2-Chloro-1-(chloromethyl)ethyl carbamate

C4H7Cl2NO2

HCID76359

Cyclohexylidenebis(tert-butyl) peroxide

C14H28O4

$结构：CCCCCCCCCCCCCOC(=O)/C=C\C(=O)OCCCCCCCCCCCCC$

HCID6437427

Ditridecyl (2Z)-2-butenedioate

C30H56O4

PRODUCTS

生成物

$结构：CCCCCCCCCCCCCOC(=O)/C=C\C(=O)OCCCCCCCCCCCCC.NC(=O)OC(CCl)CCl$

HCID131712900

未命名化合物

CONDITIONS

反应条件

温度: 110 °C

PROCEDURE

实验过程

To a 500 ml resin kettle equipped with an overhead stirrer and containing 200 g of Flo Mo 36C (ethoxylated castor oil) were added 50 g ditridecyl maleate and 6 g 1,1-bis(t-butylperoxy) cyclohexane (available from Witco Chemical Company under the tradename USP-400P). The mixture was then heated to 110° C. for 4 hours under nitrogen to yield a viscous liquid surfactant of the invention (Surfactant No. 54).

WORKUP

后处理

customto yield a viscous liquid surfactant of the invention (Surfactant No. 54)

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-6074226a766d4fcdabb8b202d23ed75b
来源数据集: uspto-grants-1988_03
DOI: 10.6084/m9.figshare.5104873.v1
专利: US04729850
来源说明: uspto-grants-1988_03

反应 SMILES

[CH2:1]([Cl:9])[CH:2]([O:5][C:6]([NH2:8])=[O:7])[CH2:3][Cl:4].[C:10]([O:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH3:43])(=[O:29])/[CH:11]=[CH:12]\[C:13]([O:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28])=[O:14].C(OOC1(OOC(C)(C)C)CCCCC1)(C)(C)C>>[CH2:1]([Cl:9])[CH:2]([O:5][C:6]([NH2:8])=[O:7])[CH2:3][Cl:4].[C:13]([O:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28])(=[O:14])/[CH:12]=[CH:11]\[C:10]([O:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH3:43])=[O:29]