HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Propanol → HCID 4713437, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Propanol | HCID 1031 | — |
| Reactant | 3-Aminonorharman | HCID 119537 | — |
| Product | HCID 4713437 | HCID 4713437 | — |
Reaction Steps
184 mg of 3-amino-β-carboline are mixed with 0.5 ml of i-amylnitrite in 15 ml of n-propanol at room temperature and stirred for 15 minutes. Then it is heated for 4.5 hours to 80° C. bath temperature. After concentration, it is chromatographed on silica gel with methylene/chloride/acetone=1:1 as eluant. After concentration and recrystallization of the corresponding fractions from diisopropyl ether/cyclohexane, 120 mg of 3-propoxy-β-carboline with a 147°-151° C. melting point are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04731358 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-8d676f35f0b1479199a38ca2fa54eec6 |
| Source note | uspto-grants-1988_03 |