HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitromethane → HCID 54347464, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Methylamine hydrochloride | HCID 6364545 | — |
| Reactant | HCID 54371401 | HCID 54371401 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54347464 | HCID 54347464 | — |
Reaction Steps
A solution of 5-formyl-4-methyl-beta-carboline-3-carboxylic acid ethyl ester (10 g), nitromethane (2 ml) and methylamine hydrochloride (0.2 g) in ethanol (50 ml) is mixed with sodium carbonate (0.3 g) and left for 5 days at 20° C. with occasional shaking. Then it is evaporated to beginning crystallization. 5 g of the title compound crystallizers from the solution cooled with ice water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04731365 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-c742e44923574d4bb065a15fa09ccb60 |
| Source note | uspto-grants-1988_03 |