HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18612293, compound → HCID 18612289, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18612293 | HCID 18612293 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium monoxide | HCID 5083724 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 18612289 | HCID 18612289 | — |
Reaction Steps
A solution of 0.4 g of (R)-2-O-benzyl-1-O-(4-chlorobutyryl)-3-O-octadecylglycerine in 20 ml of glacial acetic acid is treated with 0.120 g of palladium oxide and hydrogen. The catalyst is removed by filtration under suction and the filtrate is dried under reduced pressure. There is obtained (R)-1-O-(4-chlorobutyryl)-3-O-octadecylglycerine of melting point 48° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04731373 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-0b143eec755845188a7ad5af7ec56857 |
| Source note | uspto-grants-1988_03 |