HuagongsheHuagongshe Chemistry Print Report · For research reference only
(E)-3-[4-(pyridin-3-ylmethyl)phenyl]allyl alcohol → 3-[4-(Pyridin-3-ylmethyl)phenyl]propanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (E)-3-[4-(pyridin-3-ylmethyl)phenyl]allyl alcohol | HCID 15594566 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-[4-(Pyridin-3-ylmethyl)phenyl]propanol | HCID 13822780 | 99.1% |
Reaction Steps
In 10 ml of ethanol was dissolved 500 mg of (E)-3-[4-(pyridin-3-ylmethyl)phenyl]allyl alcohol, and to the resulting solution was added 100 mg of 5% palladium-carbon, and the resulting mixture was stirred at room temperature in a hydrogen atmosphere for 2.5 hours. The reaction mixture thus obtained was filtered and the filtrate thus obtained was concentrated under reduced pressure to obtain 500 mg (yield 99.1%) of colorless, oily 3-[4-(pyridin-3-ylmethyl)phenyl]propanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04731370 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-8d428bae1cf941c2bd3464f16b9f2628 |
| Source note | uspto-grants-1988_03 |