HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron, trifluoro(methanol)-, (T-4)- → Methyl 2-(3-methoxyphenyl)-5-oxo-1-phenylpyrrolidin-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron, trifluoro(methanol)-, (T-4)- | HCID 11062313 | — |
| Reactant | 2-(3-Methoxyphenyl)-5-oxo-1-phenylpyrrolidin-3-carboxylic acid | HCID 13361985 | — |
| Product | Methyl 2-(3-methoxyphenyl)-5-oxo-1-phenylpyrrolidin-3-carboxylate | HCID 13362002 | — |
Reaction Steps
A solution of 25.0 gm. of 2-(3-methoxyphenyl)-5-oxo-1-phenylpyrrolidin-3-carboxylic acid in 200 ml 10-15% boron fluoride-methanol was refluxed for 8 hours and upon following the workup for example 1C the product was obtained as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04731457 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-999296dc3304461a8deb656b3ad85617 |
| Source note | uspto-grants-1988_03 |