HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → 2-Methoxy-1-naphthylidene-phenylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 2-Methoxy-1-naphthaldehyde | HCID 79352 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 2-Methoxy-1-naphthylidene-phenylamine | HCID 20148843 | 102.2% |
Reaction Steps
2-Methoxy-1-naphthaldehyde [50.0 gm. 0.27 mole] and phenylamine [25 gm., 0.27 mole] were refluxed with benzene [100 ml] for 4 hours. The benzene was evaporated to an oil, dissolved in chloroform, the chloroform dried over sodium sulfate and evaporated to a green semi-solid of the 2-methoxy-1-naphthylidene-phenylamine [68.8 gm., 97% yield]
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04731457 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-ab20b17bbc0f41cc88cebce9f28f81c7 |
| Source note | uspto-grants-1988_03 |