Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 3-Methoxybenzaldehyde | HCID 11569 | — |
| Reactant | 3-(4-chlorophenyl)dihydrofuran-2,5-dione | HCID 289469 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 13361996 | HCID 13361996 | — |
Reaction Steps
6.3 g (0.03 mole) of (4-chlorophenyl)-succinic anhydride and 6.75 g (0.03 mole) of Schiff base, prepared from 3-methoxybenzaldehyde and benzylamine, according to the general procedure, are refluxed at 140° C. in 90 ml of xylene for 12 hr. After cooling to 0° C. the solid is collected, washed with xylene and ether: 9.15 g (70%) of title compound mp 76°-8° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04731457 |
|---|
| Source dataset | uspto-grants-1988_03 |
|---|
| ORD ID | ord-24573f4043934e5794eb02b86b07db25 |
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| Source note | uspto-grants-1988_03 |
|---|
