HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → 1-[5-Methyl-2-(2-pyridinyl)-1H-imidazol-4-yl]ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | 2-Pyridinemethanamine | HCID 19509 | — |
| Reactant | 2,3,4-Pentanetrione | HCID 136703 | — |
| Product | 1-[5-Methyl-2-(2-pyridinyl)-1H-imidazol-4-yl]ethanone | HCID 13387937 | — |
Reaction Steps
A mixture of 6.5 g of 2,3,4-pentanetrione, 3-oxime and 6.0 g of 2-pyridylmethylamine in 125 ml of acetonitrile was reacted as described in Example 1, giving 3.6 g of the desired compound, mp 145°-147° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04732895 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-c3f7afec9d5f4a309515150c801f0489 |
| Source note | uspto-grants-1988_03 |