HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 22165487, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 7-Chloro-2-tetralone | HCID 4065216 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 22165487 | HCID 22165487 | — |
Reaction Steps
11.0 g of 7-chloro-3,4-dihydro-2(1H)-naphthalenone was boiled at reflux for 2 hours in 200 ml of benzene and 6.0 ml of pyrrolidine in the presence of 0.25 g of p-toluenesulphonic acid. The 1-(7-chloro-3,4-dihydro-2-naphthyl)pyrrolidine obtained was recrystallized from 150 ml of isopropyl ether and exhibits a melting point of 115°-116°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04732979 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-e30ce85964cc4bdab416a912bb53033e |
| Source note | uspto-grants-1988_03 |