HRID569680

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID949

N,N-Dimethylaniline

C8H11N

反应SMILES：CN(C)c1ccc(C2OC(=O)c3cc(N(C)C)ccc32)cc1

HCID93693

1(3H)-Isobenzofuranone, 6-(dimethylamino)-3-[4-(dimethylamino)phenyl]-

C18H20N2O2

PRODUCTS

产物

反应SMILES：CN(C)c1ccc(C(c2ccc(N(C)C)cc2)c2ccc(N(C)C)cc2C(=O)O)cc1

HCID102063

Benzoic acid, 2-[bis[4-(dimethylamino)phenyl]methyl]-5-(dimethylamino)-

C26H31N3O2

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID3007855

Zinc chloride

Cl2Zn

PROCEDURE

实验过程

Following a procedure similar to that described in part A above, but substituting 18.2 g of anhydrous stannic chloride for the anhydrous zinc chloride, 70.0 ml of N,N-dimethylaniline and 14.9 g of 3-(4-dimethylaminophenyl)-6-dimethylaminophthalide prepared as described in Example 1, part A above were interacted to obtain 15.0 g of 2-[4,4'-bis(dimethylamino)-benzhydryl]-5-dimethylaminobenzoic acid which melted at 208°-212° C.

WORKUP

后处理

customprepared