Formaldehyde → HCID 20146070, compound

HRID 569711Notes

Reaction equation

HRID 569711 reaction equation
[NH:1]1[CH:5]=[CH:4][N:3]=[N:2]1.[CH2:6]([NH:10][CH2:11][CH2:12][CH2:13][CH3:14])[CH2:7][CH2:8][CH3:9].[CH2:15]=O>CO>[CH2:6]([N:10]([CH2:15][N:1]1[CH:5]=[CH:4][N:3]=[N:2]1)[CH2:11][CH2:12][CH2:13][CH3:14])[CH2:7][CH2:8][CH3:9]

Participants

5

Reactant 3

HCID 712FormaldehydeHCID 8148DibutylamineHCID 178418936HCID 178418936, compound

Product 1

HCID 20146070HCID 20146070, compoundYield 97%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

7 parts of triazole and 12.9 parts of di-n-butylamine and 8.1 parts of 37% aqueous formaldehyde mixed with 100 parts of methanol, are reacted as in Example 1 to provide 20.4 parts (97% yield) 1-di-n-butylaminomethyltriazole. Boiling point 105° C./0.075 m bar.

Workup

  1. customare reacted as in Example 1

Sources & evidence

ORD record
ord-f16610df3375497a92d0b5abe72b21da
Source dataset
uspto-grants-1988_03
Patent number
US04734209

Reaction notes

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