Sodium hydride → HCID 22837354, compound

Participants

Reaction Steps

Using a similar procedure to that described in Example 1(h), 1.21 g of 3(S*)-azido-6(S*)-phenylperhydroazepin-2-one (Isomer B) [prepared as described in Example 1(g)], 1 ml of t-butyl bromoacetate and 252 mg of sodium hydride (as a 55% w/w dispersion in mineral oil) afforded 1.9 g of the title compound as a syrup.

Provenance & Evidence