Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 14698107 | HCID 14698107 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 14698108 | HCID 14698108 | — |
Reaction Steps
Hydrogen peroxude (1 equivalent, 30%) is added to a solution of 4-methyl-5-[4-(methylthio)benzoyl)-2(3H)-thiazolone (2.7 g) in glacial acetic acid (80 ml). The mixture is stirred for 3 hours at 50° C. The precipatate obtained on addition of water is recrystallized from ethanol to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04734422 |
|---|
| Source dataset | uspto-grants-1988_03 |
|---|
| ORD ID | ord-0466d3f684744909975af47551b493ad |
|---|
| Source note | uspto-grants-1988_03 |
|---|
