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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 569795Generated: October 29, 2026

Hexamethyldisiloxane → HCID 20146228, compound

https://huagongshe.com/reaction/569795

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHexamethyldisiloxaneHCID 24764—
ReactantHCID 13687911HCID 13687911—
ReactantEthylacetate methanolHCID 21584119—
ProductHCID 20146228HCID 20146228—

Reaction Steps

Methyl 6-[1-hydroxy-1-phenyl-1-(3-pyridyl)methyl]-2-naphthoate is prepared from 2-acetyl-6-(1-hydroxy-1-phenyl-1-(3-pyridyl) methyl)naphthalene in analogy to 3a without intermediate protection of the hydroxyl group as the trimethylsilyl ether. RF (ethyl acetate/methanol): 0.53.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04734406
Source datasetuspto-grants-1988_03
ORD IDord-bf671d240ac54ae49d888966796c9770
Source noteuspto-grants-1988_03