HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 20142835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Benzenepentanoic acid | HCID 16757 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | Glycine ethyl ester, hydrochloride | HCID 2723640 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20142835 | HCID 20142835 | — |
Reaction Steps
5-Phenylvaleric acid (2.67 g, 15 mmol) in distilled THF was reacted with CDI (15 mmol) followed by glycine ethyl ester·HCl (15 mmol) and (C2H5)3N (15 mmol) as described in Example 56 Part A. The crude material (3.25 g, 82%) was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04734426 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-ff21d3651b82456fa8b8142ba8f37e82 |
| Source note | uspto-grants-1988_03 |